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Possible Spoilers
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Relax matey, there are many tactics to employ here. Firstly, when he becomes demi-lich form, he has 2 main attacks. The Demi-Lich howl and imprisionment. Counteract the first using a deathward spell on your tank, and the second can be avoided by a number of ways. If you have a berserker or Minsc, then enrage (barbarian rage does not work however). Otherwise, employ your mage with spell immunity in abjuration (your best bet), or spell trap (which will absorb about 3 imprisionments before you're boned). You can only hit him with +4 and above weapons, and use improve haste to double your attacks. Ring of the Ram does damage him too (and if you pick pocketed Tolgerias in the government district then you will have 2 of them!) so you can take a good 15-20 damage of his HP then (think he has 50 in this form). Demi-Liches have 100% magic resistance and 90% resistance to all forms of physical damage so you need to hit him hard and fast. Hope this helps.
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